期刊信息

  • 刊名: 河北师范大学学报(自然科学版)Journal of Hebei Normal University (Natural Science)
  • 主办: 河北师范大学
  • ISSN: 1000-5854
  • CN: 13-1061/N
  • 中国科技核心期刊
  • 中国期刊方阵入选期刊
  • 中国高校优秀科技期刊
  • 华北优秀期刊
  • 河北省优秀科技期刊

3-磺酸基对茴香胺合成中溶剂的选择

  • 石家庄职业技术学院 化工系 河北 石家庄 050016
  • DOI:

The Solvents Selection on the Synthesis of 3-sulfo p-anisidine

摘要/Abstract

摘要:

用溶剂汽油、萘烷、石油醚按一定比例复配成混合型溶剂,以对茴香胺为原料,用该溶剂合成了3磺酸基对茴香胺,产品中不含致癌物.产品收率在82%以上,溶剂回收率在95%以上.

Abstract:

The mixed solvent consists of solvent naphtha , decalin , and petroleum ether in a certain proportion , which was used to synthesize 3-sulfo p-anisidine by using p-anisidine as raw material .The yield ofprouduct was over 82 %, and there was no carcinogenic compound in the product , and the recovery of solvent was over 95 %.