期刊信息

  • 刊名: 河北师范大学学报(自然科学版)Journal of Hebei Normal University (Natural Science)
  • 主办: 河北师范大学
  • ISSN: 1000-5854
  • CN: 13-1061/N
  • 中国科技核心期刊
  • 中国期刊方阵入选期刊
  • 中国高校优秀科技期刊
  • 华北优秀期刊
  • 河北省优秀科技期刊

加替沙星的吸附伏安特性及其应用

  • 渭南师范学院化学化工系, 陕西渭南 714000
  • DOI:

Adsorptive Voltammetric Behavior of Gatifloxacin and Its Application

摘要/Abstract

摘要:

在0.3 mol/L KH2PO4-NaH2PO4(pH6.4)底液中,加替沙星(GTF)在汞电极上的线性扫描伏安测试显示一个还原峰,并具有明显的吸附特性,测得GTF在汞电极上的饱和吸附量为40.1 pmol/cm2.GTF在汞电极上的吸附符合Langmuir吸附等温式,建立了吸附溶出伏安法测定GTF的最佳条件,方法的检出限为20.0 nmol/L.

Abstract:

In a supporting electrolyte of 0.3 mol/L KH2PO4-NaH2PO4(pH6.4),a reduction peak of Gatifloxacin(GTF) adsorptive characteristics at Hg electrode was observed by linear sweep voltammetry.The saturated adsorption amount was 40.1 pmol/cm2.On the surface of the hanging mercury drop electrode,the adsorption obeyed langmuir adsorption isotherm.A method for the assay of GTF was proposed by adsorptive stripping voltammetry.The detection limit of the method is 20.0 nmol/L under the optimized conditions.