在线阅读 --自然科学版 2012年1期《伊潘立酮的NMR谱研究》
伊潘立酮的NMR谱研究--[在线阅读]
刘英华1, 尚振华2, 赵晓丹2, 胡硕2, 原现瑞1
1. 河北科技大学河北省分析测试研究中心, 河北石家庄050018;
2. 河北科技大学化学与制药工程学院, 河北石家庄050018
起止页码: 62--66页
DOI:
摘要
对伊潘立酮的一维和二维核磁共振谱(1HNMR,19FNMR,13CNMR,DEPT,1H-1HCOSY,HSQC,HM-BC)进行了解析,对1H,13CNMR信号进行了归属,确证了伊潘立酮的结构.

Structure Elucidation of Iloperdone by NMR Spectra
LIU Yinghua1, SHANG Zhenhua2, ZHAO Xiaodan2, HU Shuo2, YUAN Xianrui1
1. Hebei Research Center of Analysis and Testing, Hebei University of Science and Technology, Hebei Shijiazhuang 050018, China;
2. College of Chemical and Pharmaceutical Engineering, Hebei University of Science and Technology, Hebei Shijiazhuang 050018, China
Abstract:
The 1D and 2D NMR(1HNMR,19FNMR,13CNMR,DEPT,1H-1HCOSY,HSQC and HMBC) spectra of iloperidone were reported and interpreted.1H,133CNMR signals were assigned.The structure of iloperidone was elucidated.

收稿日期: 2011-4-26
基金项目: “十二五”重大新药创制专项基金(2011ZX09202-101-22)

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