在线阅读 --自然科学版 2009年1期《7-甲基吲哚啉合成新工艺》
7-甲基吲哚啉合成新工艺--[在线阅读]
张宝华1, 史兰香2, 岳红坤2, 朱云云2
1. 石家庄学院物理系, 河北石家庄050035;
2. 石家庄学院化工学院, 河北石家庄050035
起止页码: 83--84页
DOI:
摘要
报道了以7-甲基吲哚为原料,用Zn-AlCl3.6H2O-H2O还原体系在回流状态下制备了7-甲基吲哚啉的一种新工艺.当n(7-甲基吲哚):n(Zn):n(AlCl3.6H2O)=1:1.5:0.05时,产物收率达92%.

The New Synthesis Method of 7-methylindoline
ZHANG Bao-hua1, SHI Lan-xiang2, YUE Hong-kun2, ZHU Yun-yun2
1. Department of Physics, Shijiazhuang University, Hebei Shijiazhuang 050035, China;
2. College of Chemical Engineering, Shijiazhuang University, Hebei Shijiazhuang 050035, China
Abstract:
The new method of preparing 7-methylindoline by reduction of 7-methy lindole with Zn-AlCl3#6H 2O-H2O at reflux was described.While n(7-methylindole):n(Zn):n(AlCl3#6H2O)=1:1.5:0.05,they ield of product was up to 92%.

收稿日期: 2008-3-20
基金项目: 河北省科学技术厅科学研究基金(07215603D)

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